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Effects of supercritical carbon dioxide on crystallisation behaviour of polycarbonate/poly (methyl methacrylate) blends

SnCl2·2H2O-modified polycarbonate (PC)/poly(methyl methacrylate) (PMMA) (80/20 w/w) blends were prepared by melt blending using a torque rheometer. Supercritical carbon dioxide (scCO2) has been used to induce the crystallisation of PC/PMMA blends while the crystallisation behaviour and morphology of... Full description

Contained in: Plastics, Rubber and Composites Vol. 45, No. 9 (2016), p. 407-414
Journal Title: Plastics, Rubber and Composites
Fulltext access:
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Links: Additional Link (dx.doi.org)
ISSN: 1743-2898
Additional Keywords: DREHMOMENTRHEOMETER
ELEKTRONENMIKROSKOPIE
KALORIMETRIE
KRISTALLINITAET
KRISTALLISATIONSVERHALTEN
METHACRYLSAEUREMETHYLESTER
POLYCARBONAT
SAETTIGUNGSTEMPERATUR
STOFFGEMISCH
TEMPERATURERHOEHUNG
UEBERKRITISCHES-KOHLENDIOXID
DOI: 10.1080/14658011.2016.1220155
Notes: Copyright: Metadaten: TEMA, Copyright WTI-Frankfurt eG
Copyright: (C) Alle Rechte beim Herausgeber
Physical Description: 8 Seiten, 30 Quellen
ID (e.g. DOI, URN): 10.1080/14658011.2016.1220155
PPN (Catalogue-ID): WTI003428818
Note: WTI TEMA DB
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520 |a SnCl2·2H2O-modified polycarbonate (PC)/poly(methyl methacrylate) (PMMA) (80/20 w/w) blends were prepared by melt blending using a torque rheometer. Supercritical carbon dioxide (scCO2) has been used to induce the crystallisation of PC/PMMA blends while the crystallisation behaviour and morphology of these blend systems under different saturation temperatures, saturation pressures, saturation times and co-solvent contents were characterised by differential scanning calorimetry (DSC) and scanning electron microscopy (SEM). The gravimetric experiment shows that the solubility of scCO2 in PC/PMMA blends increases with the increase of saturation temperature, pressure and time. The DSC curves demonstrate that in these blend systems, the induced crystallisation of PC has been found and two kinds of crystals with different thicknesses exist in it. From the SEM images, it can be found that the structure of PC crystal becomes more perfect and its crystallinity also increases with the increase of saturation temperature, pressure, time and co-solvent content. [Taylor & Francis Group. Reproduced with permission.] 
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