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Processibility and Thermo-Mechanical Properties of Epoxy as Reactive Plasticizer of Polyetherimide

A relatively new way to improve processibility thermoplastics is via the use of crosslinkable monomers which can act as reactive plasticizers and reduce the viscosity in the early stage of processing. The monomers can polymerize and phase separate during final stage of processing thus recovering the... Full description

Published: Zürich, Trans Tech Publications, 2017
Kongresse: Scientific Conference of the Microscopy Society Malaysia 25 2016.12.07-2016.12.09 Bangi, MY
SCMSM 25 2016.12.07-2016.12.09 Bangi, MY
Scientific Conference of the Microscopy Society Malaysia 25th 2016.12.07-2016.12.09 Bangi, MY
SCMSM 2016 2016.12.07-2016.12.09 Bangi, MY
Current Trends in Materials Engineering II 2016.12.07-2016.12.09 Bangi, MY
Contained in: Solid State Phenomena Vol. 264 (2017), p. 228-231
Journal Title: Solid State Phenomena
Fulltext access:
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Links: Additional Link (dx.doi.org)
Additional Link (www.scientific.net)
ISSN: 1662-9779
Additional Keywords: ELEKTRONENMIKROSKOPIE
GLASUEBERGANGSTEMPERATUR
KALORIMETRIE
KORNGROESSE
MONOMER
PHASENMORPHOLOGIE
PHASENTRENNUNG
POLYETHERIMID
STOFFGEMISCH
THERMOPLAST
VERARBEITUNGSEIGENSCHAFT
WEICHMACHER
DOI: 10.4028/www.scientific.net/SSP.264.228
Notes: Copyright: Metadaten: TEMA, Copyright WTI-Frankfurt eG
Copyright: (C) Alle Rechte beim Herausgeber
Physical Description: 4 Seiten
ID (e.g. DOI, URN): 10.4028/www.scientific.net/SSP.264.228
PPN (Catalogue-ID): WTI00598310X
Note: WTI TEMA DB
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520 |a A relatively new way to improve processibility thermoplastics is via the use of crosslinkable monomers which can act as reactive plasticizers and reduce the viscosity in the early stage of processing. The monomers can polymerize and phase separate during final stage of processing thus recovering the original thermoplastics properties. In this work, the applicability of epoxy as reactive plasticizer for polyetherimide (PEI) was investigated. The properties of PEI/epoxy blends without and with curative were studied in order to determine the effect of the monomer on the processibility of the PEI and the thermo-mechanical properties of cured blends. Differential Scanning Calorimetry on blends without curative indicated single glass transition temperature (Tg) at high PEI content suggesting miscibility of the system and plasticization of PEI in the presence of epoxy while cured blends indicated two Tg due to phase separation. Scanning electron microscopy of the cured blends indicated two phase morphology with PEI dispersed particles size increased in continuous epoxy matrix with increasing PEI (up to 30wt% PEI). In blends with 40wt% PEI and more, phase inverted morphology was observed where increasing PEI content caused reduction of epoxy particle size in continuous PEI matrix. [Copyright Trans Tech Publications. Reproduced with permission.] 
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