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Synthesis of polyethylene-graft-poly(styrene-co-maleic anhydride) and its compatibilizing effects on polyethylene/starch blends : Synthese von Polyethylen-Propf-Poly(styrol-co-maleinsäureanhydrid) und Untersuchung seiner Kompatibilisierungseffekte auf Polyethylen/Stärke-Mischungen

Low density polyethylen (LDPE) was reacted with benzoyl peroxid (BPO) and 2,2,6,6-tetramethyl-1-piperidinyloxy(TEMPO) to prepare a latent macroinitiator, PE-TEMPO. Little polymer was synthesized when maleic anhydride (MAH) was bulk polymerized in the presence of the PE-TEMPO. However, addition of st... Full description

Contained in: Journal of Applied Polymer Science Vol. 88, No. 10 (2003), p. 2434-2438
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Links: Additional Link (dx.doi.org)
ISSN: 1097-4628
Additional Keywords: COPOLYMER
PFROPFCOPOLYMER
POLYETHYLEN
STAERKE:POLYSACCHARID
STOFFGEMISCH
SYNTHESE
DOI: 10.1002/app.2370
Notes: Copyright: Metadaten: TEMA, Copyright WTI-Frankfurt eG
Copyright: (C) Alle Rechte beim Herausgeber
Physical Description: 5 Seiten, 4 Bilder, 2 Tabellen, 13 Quellen
ID (e.g. DOI, URN): 10.1002/app.2370
PPN (Catalogue-ID): WTI040343251
Note: WTI TEMA DB
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520 |a Low density polyethylen (LDPE) was reacted with benzoyl peroxid (BPO) and 2,2,6,6-tetramethyl-1-piperidinyloxy(TEMPO) to prepare a latent macroinitiator, PE-TEMPO. Little polymer was synthesized when maleic anhydride (MAH) was bulk polymerized in the presence of the PE-TEMPO. However, addition of styrene accelerated the polymerization rate and PE-grafted poly(styrene-co-maleic anhydride) (PE-g-P(ST-co-MAH)) was produced to a high yield. Chemical reaction between MAH units and hydroxyl groups of starch was nearly undetectable in the PE/PE-g-P(ST-co-MAH)/starch blend system, and the tensile properties of the blend were not enhanced significantly. However, addition of tetrabutyl titanate (TNBT) during the blending procedure improved the tensile properties significantly through an increased interfacial adhesion between the components in the blend system. [Copyright John Wiley & Sons. Reproduced with permission.] 
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