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Synthesis and Structural Characterization of Nanoscale BaTiO3 Powders

Nanoscale BaTiO3 powders were prepared by hydro-thermal synthesis as a function of solvent conditions. The size of the BaTiO3 powders was in the range of 20 ~ 100 nm. The variation in the relative volume fraction of the tetragonal phase was analyzed quantitatively by means of XRD and Raman spectrosc... Full description

Contained in: Materials Science Forum Vol. 558-559 (2007), p. S.1323-1327
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Links: Additional Link (dx.doi.org)
Additional Link (www.scientific.net)
Additional Keywords: FABRIKATIONSMITTEL
LOESEMITTEL
RESOLVER
VOLUMENFRAKTION
DOI: 10.4028/www.scientific.net/MSF.558-559.1323
Notes: Copyright: Metadaten: TEMA, Copyright WTI-Frankfurt eG
Copyright: Trans Tech Publications
Physical Description: 5 Seiten
ID (e.g. DOI, URN): 10.4028/www.scientific.net/MSF.558-559.1323
PPN (Catalogue-ID): WTI04921487X
Note: WTI TEMA DB
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520 |a Nanoscale BaTiO3 powders were prepared by hydro-thermal synthesis as a function of solvent conditions. The size of the BaTiO3 powders was in the range of 20 ~ 100 nm. The variation in the relative volume fraction of the tetragonal phase was analyzed quantitatively by means of XRD and Raman spectroscopy. It was found that the maximum volume fraction of the tetragonal phase was ~ 29 %; this was obtained when the synthesis was performed at a solvent condition R (H2O/(H2O + EtOH)) = 0.25. [Copyright Trans Tech Publications. Reproduced with permission.] 
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