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Hybrid Organic-Inorganic Membranes on Porous Supports by Size Exclusion and Thermal Sintering of Fluorescent Polyphenylsilsesquioxane Nanoparticles

Hybrid organic–inorganic membranes were prepared by size-exclusion deposition and thermal sintering of fluorescent polyphenylsilsesquioxane nanoparticles on a ceramic support. Fluorescent polyphenylsilsesquioxane particles were prepared by a two-step co-polymerization of phenyltriethoxysilane with 0... Full description

Contained in: Macromolecular Materials and Engineering Vol. 298, No. 7 (2013), p. 715-721
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Links: Additional Link (dx.doi.org)
ISSN: 1439-2054
Additional Keywords: DECKSCHICHT
FLUORESZENZ
KERAMIK
MEMBRAN
NANOPARTIKEL
POROSITAET
SEITENGRUPPE
SILICON:POLYMER
SINTERTECHNIK
TEILCHENABSCHEIDUNG
DOI: 10.1002/mame.201200091
Notes: Copyright: Metadaten: TEMA, Copyright WTI-Frankfurt eG
Copyright: (C) Alle Rechte beim Herausgeber
Physical Description: 7 Seiten, 8 Bilder, 15 Quellen
ID (e.g. DOI, URN): 10.1002/mame.201200091
PPN (Catalogue-ID): WTI052009211
Note: WTI TEMA DB
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520 |a Hybrid organic–inorganic membranes were prepared by size-exclusion deposition and thermal sintering of fluorescent polyphenylsilsesquioxane nanoparticles on a ceramic support. Fluorescent polyphenylsilsesquioxane particles were prepared by a two-step co-polymerization of phenyltriethoxysilane with 0.1 mol-% N-(triethoxysilylpropyl)dansylamide. Because they were larger than the pores in the support, the particles formed a layer on top of the ceramic support that was sintered at 300 °C into a homogeneous, non-porous membrane. Fluorescence of the modified polyphenylsilsesquioxane provided a valuable tool to monitor particle deposition and assist in characterization of the membranes. [Copyright Wiley-VCH Verlag GmbH & Co. KGaA. Reproduced with permission.] 
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