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Transparent and durable SiO2-containing superhydrophobic coatings on glass

We fabricated novel superhydrophobic coatings based on SiO2 nanoparticles combined with NH2-terminated silicone (SN2) or SN2-modified polyurethane (SN2-prePU) by alternately spin-coating them onto glass slides. The final fabricated surface contained SN2/SiO2 or SN2-prePU/SiO2 bilayers. The condition... Full description

Contained in: Journal of Applied Polymer Science Vol. 132, No. 8 (2015), p. 41500/1-7
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Links: Additional Link (dx.doi.org)
ISSN: 1097-4628
Additional Keywords: BESCHICHTEN
BESCHICHTUNGSMETHODE
DOPPELSCHICHT
GLAS
KONTAKTWINKEL
NANOPARTIKEL
NUTGLAS
POLYURETHAN
SCHLEUDERBESCHICHTEN
SILICIUMDIOXID
SILICON:POLYMER
TROEPFCHEN
DOI: 10.1002/app.41500
Notes: Copyright: Metadaten: TEMA, Copyright WTI-Frankfurt eG
Copyright: (C) Alle Rechte beim Herausgeber
Physical Description: 7 Seiten
ID (e.g. DOI, URN): 10.1002/app.41500
PPN (Catalogue-ID): WTI055991521
Note: WTI TEMA DB
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520 |a We fabricated novel superhydrophobic coatings based on SiO2 nanoparticles combined with NH2-terminated silicone (SN2) or SN2-modified polyurethane (SN2-prePU) by alternately spin-coating them onto glass slides. The final fabricated surface contained SN2/SiO2 or SN2-prePU/SiO2 bilayers. The conditions of spin-coating method were also explored. SN2-prePU with different SN2/prePU molar ratios were synthesized to study the influence of SN2 ratio on the water contact angles of ultimate spin-coated surfaces. The surface was found to be tunable from hydrophobic to superhydrophobic by choosing SN2-prePU with different SN2/prePU molar ratios or SN2 content. Water droplets easily rolled off on these superhydrophobic surfaces. Surfaces coated with SN2/SiO2 bilayers showed better transparency, whereas surfaces coated with SN2-prePU(2: 1)/SiO2 bilayers exhibited better durability. Droplets of varied pH were prepared to test the anti-wettability of the coatings. Results showed that the as-coated surfaces had stable superhydrophobicity to droplets with pH values ranging from 1 to 14. [Copyright John Wiley & Sons. Reproduced with permission.] 
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