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Reinforcement of polysiloxane/silica elastomer composite by introduction of sacrificial bonds

It is a challenge to improve tear strength of silicone rubber, especially at high filler loading circumstances. A method is offered here to introduce sacrificial bonds into the system. In particular, amide group was introduced onto the phenyl group of monomer methyl phenyl cyclosiloxane (DnPh) first... Full description

Contained in: Journal of Applied Polymer Science Vol. 135, No. 15 (2018), p. 46129/1-13
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Links: Additional Link (dx.doi.org)
ISSN: 1097-4628
Additional Keywords: AMIDE
COPOLYMER
COPOLYMERISATION
ELASTOMER
GUMMI
MONOMER
PHENYLGRUPPE
POLYDIMETHYLSILOXAN
REISSFESTIGKEIT
RHEOLOGIE
SILICIUMDIOXID
SILICON:POLYMER
SILICONKAUTSCHUK
VERBUNDWERKSTOFF
DOI: 10.1002/app.46129
Notes: Copyright: Metadaten: TEMA, Copyright WTI-Frankfurt eG
Copyright: (C) Alle Rechte beim Herausgeber
Physical Description: 13 Seiten, 15 Bilder, 2 Tabellen
ID (e.g. DOI, URN): 10.1002/app.46129
PPN (Catalogue-ID): WTI058079653
Note: WTI TEMA DB
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520 |a It is a challenge to improve tear strength of silicone rubber, especially at high filler loading circumstances. A method is offered here to introduce sacrificial bonds into the system. In particular, amide group was introduced onto the phenyl group of monomer methyl phenyl cyclosiloxane (DnPh) first, and this functionalized monomer (DnPh-amide) was further used for copolymerization with octamethylcyclotetrasiloxane (D4) and 2,4,6,8-tetravinyl-2,4,6,8-tetramethyl-cyclotetrasiloxane (D4Vi). Vulcanizates composed by this new copolymer (1A-50) which amide group-containing is 1 wt% and with 50 phr TS-530 exhibit high tear strength of about 54 N • mm−1, which is three times higher than that composed by polydimethylsiloxane (PDMS)/TS-530 (50 phr). The mechanical test indicates this new copolymer a promising candidate for the construction of high tear resistant silicone rubber, especially at high filler loading circumstances. [Copyright John Wiley & Sons. Reproduced with permission.] 
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